Laboratory Testing & General Mineral Processing Engineering

Laboratory Testing & General Mineral Processing Engineering

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Scale up factors (4 replies)

C
Chewe
6 years ago
Chewe 6 years ago

Good morning. My question concerns how to determine scale up factor of agitation leaching vessel in a leaching cascade. I'm doing leach tests for cobalt recovery from slag but the problem is in a batch vessel i'm using in the lab i have observed some dead zones so i wanted to propose a leaching cascade to maximize residence time. I'm working with 500g of material. How can i determine what scale up factor to use for pilot tests?

Thank you

A
Rheomet
6 years ago
Rheomet 6 years ago
2 likes by Chewe and David
  1. Determine your batch residence time at the given solids content, measure the pulp density (initial, final);
  2. Calculate the required total reactor volume for continuous test V(L) =  R(h)*F(L/h), apply the required safety factor (1.2 minimum, more if heavy frothing);
  3. Decide on the number of tanks, use baffles, test mixers with water, use decent diameter down-comers, reach to the bottom best, design carefully around this detail.

Good luck.

C
Chewe
6 years ago
Chewe 6 years ago

Thank you rheomet for the response.

T
Todd H
6 years ago
Todd H 6 years ago
2 likes by Chewe and David

Building on what Rheomet provided - In the ultimate design the number of tanks should not be less than 2 and ideally 4 or more to make sure that you minimize short circuiting.

I have done a lot of stirred tank leach tests at lab scale using nothing more than a mixer in a 1 liter beaker with good results, baffles are nice to have but not necessary if you can keep everything in suspension with mixer speed. 

Keep in mind that in a pilot plant it is good try and mimic the final plant design as closely as possible so that scale up issues are decreased.  Cascade or overflow is hard at the pilot scale if the tanks are small (<20 l) due to the fact that small overflows tend to not work well.  I have used peristaltic pumps in between stages to transfer slurry in batches down the line - can be manually controlled. 

Hope this helps.

 

Todd Harvey - Global Resource Engineering http://www.global-resource-eng.com

C
Chewe
6 years ago
Chewe 6 years ago

Thanks Todd. I have also observed that material gets stuck behind the baffles. Which makes me wonder if they're really that relevant if you can achieve a perfect solid suspension. The idea of using pump for slurry transfer looks good and i'll definitely consider it. Thank you

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