A study of some variables affecting the recovery of molybdenum from oxidized molybdenum minerals was made. The effects of variations in contact time, temperature, pulp density, particle size, and solvent concentration on the recovery of molybdenum using acid and alkaline solvents were investigated. Chemical analyses, screen analyses and microscopic examinations were made and the presence of important elements determined.
Description of the Ore
Geologically, this ore occurs in the bottom of the Chadron formation sandstone at the disconformity between the Chadron formation and the Pierre shale. Hand samples of the mineral ilsemannite have also been recovered from this deposit. The rock is composed predominantly of silica sand. The bonding material contains the molybdenum minerals and the iron minerals hydrated and otherwise.
The ore sample was stage crushed through 6 mesh and mixed by recombining splits from a Jones riffle. Upon further sampling and analysis it developed that we could cut reproducible (± 0.01% M0O3) samples at 100 gms wt from our minus 6 mesh aggregate.
The first sequence of tests were run to determine the effect of roasting on molybdenum extraction. A series of samples was roasted for one hour at temperatures of 100°, 200°, 300° and 400° C