Modern Assaying

Assay Laboratory Accidents

As the assayer at a mine is often called upon to relieve suffering in an emergency the following hints may prove helpful. Burns.—For dry burns apply freely a saturated solution of bicarbonate of soda, till the pain is allayed. The following may be used and is also applicable to scalds: Apply a mixture of bicarbonate … Read more

Retorting Amalgam & Melting Bullion

It sometimes falls to the lot of the assayer doing commercial work or working in a mining camp to retort the amalgam taken from the plates of a stamp mill and melt the resultant sponge of gold and silver into a bar, and assay the bar so the value of the product may be known. … Read more

Distilled Water for Assay Laboratory

Why Distilled Water In all operations in assaying and chemical analysis it is desirable to use distilled water. There are very few places where the assayer cannot procure distilled water. How to Purify Water for Laboratory Purposes without Distilling If it is necessary to use ordinary water, add a few drops of nitrate of silver … Read more

Volumetric Assay Copper Determination by Solution of Potassium Cyanide

The general method of assaying copper values is by what is termed the “wet” process, that is volumetric determination by titrating with standard solution of potassium cyanide. This method is very accurate when carefully done, but care must be taken to keep the standard solution at a given strength. Preparation of Sample The original sample … Read more

Gold Purity Testing

Description of Touch Stone and Test Needles The touch or test stone is practically a small black whetstone. Test needles (Fig. 47) are a number of slim pointed brass fingers, one end having gold points of different fineness expressed in karats (the karat is the jeweler’s standard of measure for gold, and 24 karats is … Read more

Smelting Fluxes

General Flux In a laboratory where much work is done in a day, and the class of ore is uniform, what is called a “general smelting flux” may be made. This flux is adapted to ores that may be classified as average, but is so compounded as to allow the addition of extra litharge and … Read more

Assay Balance Scale for Weighing Samples

Analytical Balances Buy a good button balance, for should the final weighing of the gold or silver recovered from an assay charge be inaccurate, all the previous work will have been wasted. A good button balance can be purchased for $100.00 (Fig. 42); higher grades that are more sensitive and delicate of construction will cost … Read more

Fire Assay of Antimony

Usual Charge Mix 10 grams of the pulped ore with 40 grams of pulverized potassium cyanide. Melting Put the charge into a 20 gram crucible or one of equivalent capacity, and cover the top of the charge with about 10 grams of dry table salt. The salt cover prevents the charge from boiling over the … Read more

Gold Bullion Assay

Drilling Bullion Bar for Sampling Bullion submitted for assay is usually brought in the form of bars, bricks, slugs or buttons, and a sample of bullion in this form is best obtained by drilling into the brick or slug with a small bit 3/16″ in diameter (Fig. 32). Drill enough so that the shavings or … Read more

Scorification

Definition of Term Scorification: Scorification may be defined as a reduction and a partial or preliminary cupellation successively performed in the same container without removal of the container from the muffle until volatilization is stopped by the slag entirely covering the charge. When is Scorification Assay Used Scorification is the proper method of assaying copper mattes. … Read more